SEPSERV
HPLC

Separation Service Berlin
Helmholtzstr. 2 - 9, Aufg. L, D-10587 Berlin
Anfahrt/Approach

Tel.:  (030) 393 09 91    Fax: (030) 393 49 25  oder  391 01 000

E-Mail: sepserv.berlin@t-online.de  Internet: www.sepserv.de

Application PAHEFSA

Packing:

UltraSep ES PAH EFSA

Column:

125 x 3 mm

Detection:

UV 254 nm

Eluent:

Water/acetonitrile (AN),
(from the 29th minute AN+10% THF)

Gradient:

Start          40% AN
25th min   100% AN

Flow rate:

0.6 ml/min

Temperature:

25°C

Sample:

EPA/EFSA-aromatics

 

1

Naphthalene

14

Dibenz(a,h)anthracene

2

Acenaphthylene

15

Benzo(g,h,i)perylene

3

Acenaphthene

16

Indeno(1,2,3-c,d)pyrene

4

Fluorene

17*

1-Methylnaphthalene

5

Phenanthrene

18*

2-Methylnaphthalene

6

Anthracene

19*

Benzo(e)pyrene

7

Fluoranthene

20**

Cyclopenta(c,d)pyrene

8

Pyrene

21**

5-Methylchrysene

9

Benz(a)anthracene

22**

Benzo(j)fluoranthene

10

Chrysene

23**

Dibenzo(a,l)pyrene

11

Benzo(b)fluoranthene

24**

Dibenzo(a,e)pyrene

12

Benzo(k)fluoranthene

25**

Dibenzo(a,i)pyrene

13

Benzo(a)pyrene

26**

Dibenzo(a,h)pyrene

 

 

The switchover peak behind compound 24 has been suppressed.

*  Inclosed only in the extended EPA list

** Polycyclic aromatic hydrocarbons of the SCF list (EU)

 

 

 

 

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